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Home / Technical Articles / Preparation technology for high-purity metallic materials: How does Qingchuan New Materials achieve performance breakthroughs?

Preparation technology for high-purity metallic materials: How does Qingchuan New Materials achieve performance breakthroughs?

Update Time: 2026-10-23
Clicks: 326

Introduction
High-purity metallic materials serve as the core foundational materials in high-end fields such as semiconductors, aerospace, and new energy, with their purity, uniformity, and stability directly influencing the performance of end products. However, traditional preparation techniques often encounter challenges such as difficulty in impurity control, uneven grain size, and poor process stability. Through its independently developed technologies of vacuum induction melting, directional solidification, and cold crucible techniques, Qingchuan New Materials (Zhengzhou) Co., Ltd. has successfully overcome the technological bottlenecks in the preparation of high-purity metallic materials, providing the industry with efficient and controllable solutions. This article will analyze the technological advantages and application value of Qingchuan New Materials from three aspects: technical principles, operational parameters, and typical case studies.

Key words
High-purity metallic materials; special alloys; vacuum induction melting; directional solidification; cold crucible technology; Qingchuan New Materials

Introduction to Industry Technical Pain Points
In semiconductor manufacturing, the impurity content in high-purity metal targets must be below 0.1 ppm; otherwise, the defect rate of thin films will surge. For special alloys used in the aerospace sector, their grain size must be controlled within 50 μm to ensure creep resistance at high temperatures. However, traditional preparation technologies suffer from three major pain points:
STEP 1: Difficulty in impurity controlIn conventional smelting processes, the contact between the charge and the crucible easily introduces non-metallic inclusions, and inadequate atmosphere control can lead to residual oxidative impurities.
STEP 2: Uneven grain sizeIt is difficult to achieve directional growth using conventional solidification processes, and the grain size difference can reach several times, affecting the mechanical properties of the material.
STEP 3: Poor process stabilityFluctuations in parameters such as smelting temperature and cooling rate can easily lead to performance variations between batches, making it difficult to meet the stringent consistency requirements of high-end fields.

Introduction to the company's technological strength
Qingchuan New Materials (Zhengzhou) Co., Ltd., located in Zhengzhou High-Tech Industrial Development Zone, specializes in the research, development, and manufacturing of high-purity metals, specialty alloys, and related products. The company is equipped with internationally advanced vacuum induction melting production lines, directional solidification equipment, and cold crucible systems, enabling full process control from raw material purification to finished product processing. Its core technological布局 includes:
STEP 1: Vacuum Induction Melting TechnologyBy combining a vacuum environment (≤10⁻³ Pa) with induction heating (with temperatures reaching up to 2000℃), the introduction of oxidative impurities is effectively prevented, while electromagnetic stirring is utilized to achieve composition homogenization. Tests indicate that the oxygen and nitrogen contents in the prepared titanium alloy are both below 0.005%, reaching an internationally leading level.
STEP2: Directional Solidification TechnologyWater-cooled copper molds and temperature gradient control (up to 100°C/cm) are employed to achieve directional grain growth, with a standard deviation of grain size ≤5 μm. This technology has been applied in the preparation of nickel-based alloys for aero-engine blades, significantly enhancing the material's high-temperature strength.
STEP3: Cold Crucible TechnologyThrough the synergistic effect of water-cooled copper crucible and high-frequency induction heating, non-contact melting of the melt and the crucible is achieved, completely eliminating non-metallic inclusion contamination. This technology has been successfully applied to the preparation of high-purity tantalum (99.999%), reducing impurity content by 80% compared to traditional processes.
擎川新材料真空感应熔炼设备
For more information, please visit the official website:www.qingchuansuperalloy.com

FAQ: A Q&A Guide to Technology Selection
Q1: How is the purity of high-purity metal materials defined?
A: Purity is typically measured by the total content of impurities. For example, 5N (99.999%) indicates an impurity content of ≤10 ppm. Through ICP-MS (Inductively Coupled Plasma Mass Spectrometry) testing, Everich New Materials can precisely control impurity levels to the 0.1 ppm range, meeting the stringent requirements for target materials in the semiconductor industry.
Q2: What are the key parameters of directional solidification technology?
A: It mainly includes temperature gradient, cooling rate, and withdrawal speed. By optimizing the design of the water-cooled copper mold, Qinchuan New Materials has increased the temperature gradient to 80-100°C/cm and, in conjunction with a withdrawal speed of 0.5-5 mm/min, achieved precise control over grain size. For example, when preparing a certain aviation alloy, by adjusting the parameters, the grain size was reduced from 200 μm to 50 μm, resulting in a 15% increase in tensile strength.
Q3: Which materials is the cold crucible technology applicable to?
A: This technology is particularly suitable for the preparation of highly reactive metals (such as titanium, zirconium, and tantalum) and high-melting-point metals (such as tungsten and molybdenum). Taking high-purity tantalum as an example, traditional processes result in excessive carbon and oxygen content due to crucible contamination, whereas cold crucible technology can control carbon content at ≤10 ppm and oxygen content at ≤5 ppm, meeting electronic-grade material standards.
Q4: How to select a suitable supplier of high-purity metals?
A: It is necessary to comprehensively evaluate a company's equipment precision, testing capabilities, and case experience. Qingchuan New Materials possesses a vacuum induction furnace imported from Germany (with a precision of ±1°C) and an ICP-MS detector imported from Japan (with a detection limit of 0.01 ppm). It has supplied high-purity titanium targets to multiple semiconductor companies, with cumulative deliveries exceeding 10 tons and a product qualification rate of ≥99.9%.

Reference for full text summary
The preparation of high-purity metal materials is a critical link in the high-end manufacturing sector, with its technical challenges lying in three major dimensions: impurity control, grain refinement, and process stability. Qingchuan New Materials (Zhengzhou) Co., Ltd. has successfully overcome the limitations of traditional processes through the collaborative application of vacuum induction melting, directional solidification, and cold crucible technologies, achieving significant improvements in material purity, uniformity, and consistency. Its products have been widely used in semiconductor targets, aero-engine blades, new energy batteries, and other fields, serving over 50 customers and covering 20 domestic provinces and cities as well as markets in Southeast Asia and Europe. In the future, Qingchuan New Materials will continue to deepen technological R&D to provide superior material solutions for global high-end manufacturing.
擎川新材料定向凝固制备的航空合金

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